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技術(shù)文章

當(dāng)前位置：首頁技術(shù)文章實(shí)驗(yàn)室氣相色譜儀是一種廣泛應(yīng)用于化學(xué)分析領(lǐng)域的儀器

實(shí)驗(yàn)室氣相色譜儀是一種廣泛應(yīng)用于化學(xué)分析領(lǐng)域的儀器

更新時(shí)間：2025-08-07

點(diǎn)擊次數(shù)：517

　　實(shí)驗(yàn)室氣相色譜儀是一種基于物質(zhì)在氣相和固定相間分配系數(shù)差異實(shí)現(xiàn)混合物分離與分析的高精度儀器，氣相色譜儀通過載氣(如氮?dú)?、氦?將氣化后的樣品帶入色譜柱，柱內(nèi)固定相對(duì)不同組分的吸附/溶解能力不同，導(dǎo)致各組分在柱內(nèi)運(yùn)行速度差異。分配系數(shù)高的組分滯留時(shí)間更長，移動(dòng)速度慢；反之則移動(dòng)快。隨著載氣不斷流過，各組分在柱中兩相間經(jīng)過反復(fù)分配與平衡，實(shí)現(xiàn)分離。分離后的組分依次進(jìn)入檢測器，轉(zhuǎn)化為電信號(hào)并被記錄為色譜峰，通過峰面積/峰高定量分析各組分含量。

　　氣相色譜儀的工作原理基于不同物質(zhì)在兩相(固定相和流動(dòng)相)間的分配平衡差異。在儀器內(nèi)部，樣品被氣化后由載氣帶入色譜柱。柱內(nèi)填充有固定相(如吸附劑、液體涂布劑等)，各組分在通過色譜柱時(shí)，由于與固定相間的相互作用力不同，導(dǎo)致在柱內(nèi)的遷移速度產(chǎn)生差異。隨著載氣的持續(xù)流動(dòng)，各組分依次從色譜柱中流出，進(jìn)入檢測器進(jìn)行檢測。檢測器將組分濃度轉(zhuǎn)換為電信號(hào)，記錄系統(tǒng)則將這些電信號(hào)繪制成色譜圖，從而反映樣品中各組分的含量和性質(zhì)。

　　設(shè)備結(jié)構(gòu)：七大模塊協(xié)同工作

　　載氣供氣系統(tǒng)：包括供氣鋼瓶、減壓穩(wěn)壓器、過濾干燥器、流量控制器等，載氣流量一般控制在10—200mL/min。

　　分離色譜柱：色譜柱是氣相色譜儀的核心，填充柱、毛細(xì)管柱和填充毛細(xì)管柱為常用類型，樣品分析的分離全靠在色譜柱中進(jìn)行。

　　進(jìn)樣系統(tǒng)：準(zhǔn)確調(diào)整每次分析的進(jìn)樣量，同時(shí)將液態(tài)樣品轉(zhuǎn)化為氣相后加入載氣氣流中，具備溫度可調(diào)的汽化器。

　　檢測器：包括熱導(dǎo)檢測器(TCD)、氫火焰離子化檢測器(FID)、電子捕獲檢測器(ECD)、質(zhì)譜檢測器(MS)等，將組分的理化特性轉(zhuǎn)化為電信號(hào)。

　　供電及信號(hào)處理系統(tǒng)：檢測器供電要求穩(wěn)定，輸出信號(hào)需經(jīng)放大后傳輸至記錄儀或數(shù)據(jù)處理裝置(如數(shù)字顯示打印自動(dòng)積分儀、小型電子計(jì)算機(jī))。

　　恒溫及程序控制系統(tǒng)：控制色譜柱、檢測器及汽化器的溫度，精度一般達(dá)±0.5℃，支持程序升溫、柱子自動(dòng)切換等功能。

　　數(shù)據(jù)處理系統(tǒng)：包括色譜工作站軟件，用于色譜圖顯示、峰積分、定量計(jì)算及報(bào)告生成。

上一條全自動(dòng)變壓器油色譜儀用于分析變壓器油中溶解氣體的組分含量
下一條解鎖氦離子化色譜儀的奧秘

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